Synthesis and structural characterization of a series of tetranuclear lanthanide clusters

dc.contributor.author Baskar, Viswanathan
dc.contributor.author Roesky, Peter W.
dc.date.accessioned 2022-03-27T09:00:18Z
dc.date.available 2022-03-27T09:00:18Z
dc.date.issued 2005-11-17
dc.description.abstract Tetranuclear lanthanide clusters of composition [Ln4(μ 3-OH)2(Ph2acac)10] (Ln = Pr, Nd, and Sm) (Ph2acac = dibenzoylmethanide) were prepared starting from [LnCl3·(n H2O)] (n = 6, 7) with 2.5 equivalents dibenzoylmethane in presence of triethylamine. Single crystals X-ray analyses of compounds 1-3 revealed that each cluster consists of four lanthanide atoms, two μ3-oxygen atoms, and ten Ph2acac ligands, which make up the peripheral part of the cluster. Three types of coordination modes (η2-, (μ-O)-η2-, and μ-O) 2-η2) are observed for the Ph2acac ligation to the metal centers. © 2005 Wiley-VCH Verlag GmbH & Co. KGaA.
dc.identifier.citation Zeitschrift fur Anorganische und Allgemeine Chemie. v.631(13-14)
dc.identifier.issn 00442313
dc.identifier.uri 10.1002/zaac.200500138
dc.identifier.uri https://onlinelibrary.wiley.com/doi/10.1002/zaac.200500138
dc.identifier.uri https://dspace.uohyd.ac.in/handle/1/12249
dc.subject Clusters
dc.subject Lanthanides
dc.subject O ligands
dc.subject Rare-earth compounds
dc.title Synthesis and structural characterization of a series of tetranuclear lanthanide clusters
dc.type Journal. Article
dspace.entity.type
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