An expedient, facile and simple one-pot synthesis of 2-methylenealkanoates and alkanenitriles from the Baylis-Hillman bromides in aqueous media.
An expedient, facile and simple one-pot synthesis of 2-methylenealkanoates and alkanenitriles from the Baylis-Hillman bromides in aqueous media.
| dc.contributor.author | Basavaiah, Deevi | |
| dc.contributor.author | Reddy, Kanumuri Ramesh | |
| dc.contributor.author | Kumaragurubaran, Nagaswamy | |
| dc.date.accessioned | 2022-03-27T09:02:03Z | |
| dc.date.available | 2022-03-27T09:02:03Z | |
| dc.date.issued | 2007-01-01 | |
| dc.description.abstract | This protocol is for an expedient and operationally simple one-pot synthesis of 2-methylenealkanoates and alkanenitriles in high yields from the corresponding Baylis-Hillman bromides. The reaction proceeds via the successive treatment with 1,4-diazabicyclo(2.2.2)octane (DABCO) for 15 min and sodium borohydride for 15 min in aqueous media [tetrahydrofuran (THF):H2O (1:1)] at room temperature. | |
| dc.identifier.citation | Nature protocols. v.2(11) | |
| dc.identifier.uri | 10.1038/nprot.2007.369 | |
| dc.identifier.uri | http://www.nature.com/articles/nprot.2007.369 | |
| dc.identifier.uri | https://dspace.uohyd.ac.in/handle/1/12302 | |
| dc.title | An expedient, facile and simple one-pot synthesis of 2-methylenealkanoates and alkanenitriles from the Baylis-Hillman bromides in aqueous media. | |
| dc.type | Journal. Article | |
| dspace.entity.type |
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