Resolution of trans-(±)-2-(pyrrolidinyl)cyclohexanol and its methyl ether using boric acid and chiral 1,1'-bi-2-naphthol
Resolution of trans-(±)-2-(pyrrolidinyl)cyclohexanol and its methyl ether using boric acid and chiral 1,1'-bi-2-naphthol
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Date
1999-06-18
Authors
Periasamy, Mariappan
Ramanathan, C. Ramaraj
Kumar, Nangunoori Sampath
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Abstract
The trans-(±)-2-(pyrrolidinyl)cyclohexanol 1, and its methyl ether 2 were resolved using chiral 1,1'-bi-2-naphthol and boric acid in THF or CH3CN. X-Ray structural analysis was carried out for the diastereomeric complex 3 obtained using 2.
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Tetrahedron Asymmetry. v.10(12)