Oxalate based non-aqueous sol-gel synthesis of phase pure sub-micron LiFePO < inf > 4 < /inf >
Oxalate based non-aqueous sol-gel synthesis of phase pure sub-micron LiFePO < inf > 4 < /inf >
| dc.contributor.author | Sundarayya, Y. | |
| dc.contributor.author | Kumara Swamy, K. C. | |
| dc.contributor.author | Sunandana, C. S. | |
| dc.date.accessioned | 2022-03-27T09:52:56Z | |
| dc.date.available | 2022-03-27T09:52:56Z | |
| dc.date.issued | 2007-11-06 | |
| dc.description.abstract | We report on the synthesis and preliminary characterisation by X-ray diffraction (XRD), scanning electron microscopy (SEM), Mössbauer spectroscopy and infrared spectroscopy (IR) of C-LiFePO4. Homogeneous sub-micron sized particles of surface carbon coated phase pure LiFePO4 are synthesised by a novel non-aqueous oxalate based sol-gel procedure. Our synthetic route successfully overcomes the incidence of Fe3+, effectively controls undesirable particle growth and has the potential for upscaling and application as Li-ion battery cathodes. © 2007 Elsevier Ltd. All rights reserved. | |
| dc.identifier.citation | Materials Research Bulletin. v.42(11) | |
| dc.identifier.issn | 00255408 | |
| dc.identifier.uri | 10.1016/j.materresbull.2006.12.006 | |
| dc.identifier.uri | https://www.sciencedirect.com/science/article/abs/pii/S0025540806004995 | |
| dc.identifier.uri | https://dspace.uohyd.ac.in/handle/1/13401 | |
| dc.subject | A. Nanostructures | |
| dc.subject | B. Sol-gel chemistry | |
| dc.subject | C. Mössbauer spectroscopy | |
| dc.subject | C. X-ray diffraction | |
| dc.title | Oxalate based non-aqueous sol-gel synthesis of phase pure sub-micron LiFePO < inf > 4 < /inf > | |
| dc.type | Journal. Article | |
| dspace.entity.type |
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