Redox shield enfolding a magnetic core

dc.contributor.author Kishore, Pilli V.V.N.
dc.contributor.author Rasamsetty, Amaleswari
dc.contributor.author Carolina Sañudo, E.
dc.contributor.author Baskar, Viswanathan
dc.date.accessioned 2022-03-27T08:59:35Z
dc.date.available 2022-03-27T08:59:35Z
dc.date.issued 2015-12-14
dc.description.abstract Ferrocenyl betadiketones were reacted with hydrated lanthanide trihalides in presence of a base to yield red color solids, whose structures were characterized by single crystal X-ray diffraction technique. Structural analysis revealed the formation of nona- and tetranuclear lanthanide oxo-hydroxo clusters [Dy9(μ4-O)2(μ3-OH)8(μ-Fca)8(Fca)8]-[HN(C2H5)3]+ (1), [Ln4(μ-OH)2(μ-OCH3)4(CH3OH)2(Fctfa)6] Ln = Yb (2), Lu (3), and [Ln4(μ-OH)2(μ-OCH3)4(CH3OH)2(Fcpfa)6] Ln = Yb (4), Lu (5). Magnetism studies revealed that 1 shows slow relaxation of magnetisation. Cyclic voltammetry studies of 1 reveal electrochemically stable quasi reversible oxidation systems whereas 2-5 showed irreversible nature.
dc.identifier.citation Polyhedron. v.102
dc.identifier.issn 02775387
dc.identifier.uri 10.1016/j.poly.2015.10.017
dc.identifier.uri https://www.sciencedirect.com/science/article/abs/pii/S0277538715005987
dc.identifier.uri https://dspace.uohyd.ac.in/handle/1/12227
dc.subject Beta-diketones
dc.subject Lanthanide oxo-hydroxo clusters
dc.subject Multi ferrocenes
dc.subject Self-assembly
dc.subject Slow relaxation of magnetization
dc.title Redox shield enfolding a magnetic core
dc.type Journal. Article
dspace.entity.type
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