Spontaneous resolution upon crystallization of allenyl-bis-phosphine oxides
Spontaneous resolution upon crystallization of allenyl-bis-phosphine oxides
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Date
2015-04-28
Authors
Gangadhararao, G.
Tulichala, R. N.Prasad
Swamy, K. C.Kumara
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Abstract
The first example of 'spontaneous resolution by crystallization' in allene chemistry, by means of crystal structures and solid state CD spectra of the R and S enantiomers, is presented. These allenes are prepared by the simple reaction of Ph2PCl with o-nitro functionalized propargyl alcohols. This journal is
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Chemical Communications. v.51(33)